Development And Validation Of Chromatographic Methods For Simultaneous Quantification Of Drugs In Bulk And In Their Formulations: HPLC And HPTLC Techniques

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1. Development and validation of a HPTLC-densitometric method for concurrent estimation of metformin hydrochloride, pioglitazone hydrochloride and gliclazide in combined dosage form.
2. Development and validation of a HPTLC method for simultaneous estimation of moxifloxacin hydrochloride and dexamethasone sodium phosphate in combined pharmaceutical dosage form.
3. Development and validation of a RP-HPLC method for simultaneous estimation of ciprofloxacin hydrochloride and dexamethasone in combined dosage form, which is a better alternative to existing ones.
The developed analytical methods are simple, selective, accurate, robust, and precise with shorter analysis time for the analysis of drug/s in combined pharmaceutical dosage forms. All the developed HPTLC and HPLC methods have been validated as per ICH Q2 (R1) guideline. Developed analytical methods could boost analytical researchers to work more efficiently in the field of analytical method development and validation of Pharmaceutical dosage forms.
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About the author

Dr. Satish Y. Gabhe, M.Pharm., Ph.D, is a Professor of Pharmaceutical Chemistry in Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune, India. He worked as a Principal in C.U. Shah College of Pharmacy, S.N.D.T. University, Mumbai. His fields of interest are Synthetic Medicinal Chemistry, Phytochemistry and Analytical Chemistry. During over 27 years of academic experience he tutored a great number of UG/ PG students and Doctoral Research Candidates. He has more than 14 international and 12 national research publications. The author has more than 45 projects completed, 6 ongoing and 3 applied patents. He received a ‘G. S. Ramaswamy Memorial’ Gold Medal for standing first in the order of merit in B. Pharm. Exam.

Dr. Kakasaheb R. Mahadik, M.Pharm., Ph.D, is a Principal and Professor of Pharmaceutical Chemistry in Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune, India. He is a member of many professional bodies of India, the American Chemical Society and the New York Academy of Sciences, USA. He is a scientific referee for several central and state government agencies. He has over 3 years of academic experience, during which he guided 22 Doctoral Research Candidates and over 76 M. Pharm. Students in the faculty of Pharmaceutical Sciences. He has published 131 international and 69 national research papers and has 22 Indian patents approved. Furthermore, he is a recipient of several scholarships and awards for his excellence in academics.

Mr. Sachin E. Potawale, M. Pharm. (Ph.D.), is pursuing his Ph.D. from Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune, India, under the guidance of Dr. Satish Y. Gabhe. Prior to that, the author completed his masters in two specializations (Pharmaceutical Chemistry and Pharmacognosy). He has one year of industrial and one year of academic experience. Currently, he is working as a Project fellow for a University Grants Commission (UGC) sponsored Special Assistance Programme. He has published 2 international and 6 national research papers and 1 review articles. He has presented several posters in various international and national seminars.

Mr. Anirudh B. Thati, M.Pharm, has completed his masters in Quality Assurance Techniques from Poona College of Pharmacy, Bharati Vidyapeeth Deemed University, Pune, India. He has also completed a certification course in Pharmacovigilance conducted mutually by Vigimedsafe and BITS Pilani, Hyderabd. Currently, ...

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Additional Information

Publisher
diplom.de
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Published on
Aug 1, 2015
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Pages
108
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ISBN
9783954898077
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Best For
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Language
English
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Genres
Science / Chemistry / Analytic
Science / Chemistry / Physical & Theoretical
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Content Protection
This content is DRM free.
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Eligible for Family Library

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TEXT BOOK MOLECULAR SPECTRA and MOLECULAR STRUCTURE I. SPECTRA OF DIATOMIC MOLECULES by GERHARD HERZBERG. Originally published in 1939. PREFACE: Eleven years ago I published a volume entitled Molecular Spectra and Molecular Structure I. Diatomic Molecules which was followed in 1945 by a second volume Infrared and Raman Spectra of Polyatomic Molecules. The first volume has been out of print for a number of years but the demand for it seemed to justify a new edition. Although the book has been completely revised and brought up to date, its general plan has remained substantially unchanged. Concerning this plan it seems therefore appropriate to quote from the preface of the first edition I have endeavored to give a presentation which is readable by the beginner in the field and also will be useful to those who do or want to do research work in this field. In order to assist the former, I have frequently made use of small type for those sections that are not necessary for an understanding of the fundamentals. For the benefit of those working in the field, numerous references to original papers have been included. A satisfactory presentation of molecular spectra and molecular structure is nowadays not possible without treating thoroughly, apart from the empirical results, the theoretical background also. Therefore I have included as much of the theory of molecular spectra as is possible without going into the more difficult mathematical details. A large number of diagrams, graphical repre sentations of eigenfunctions and potential curves, as well as energy level dia grams, serve to illustrate and to explain the theory. On the other hand, I have added numerous carefully selected spectrograms of bands and band systems some of which have been taken specially for this purpose in order to give an accurate idea of tho experimental material that forms the basis of the developments. While of course most of the material presented is not new, it seems that the actual procedure followed in analyzing a band spectrum has not previously been given as specifically in a book of this kind. The same holds for the ap plications of band spectra to other parts of physics, to chemistry, and to astro physics given in the last chapter. I hope that both these features will be found useful. In the eleven years since the publication of the first edition the subject Spectra of Diatomic Molecules has developed vigorously even though not as rapidly as in the preceding two decades. Most of the progress made has been consolidation and slow evolution rather than revolution. Exceptions to this statement are the amazing advances made by applying the new tools of molecular beams and microwaves to diatomic molecular problems. Naturally I have incorporated these advances of recent years in the present new edition...
“Telescopes and Techniques” has proved itself in its first edition, having become probably one of the most widely used astronomy texts, both for numerate amateur astronomers and for astronomy and astrophysics undergraduates. The first and second editions of the book were widely used as set texts for introductory practical astronomy courses in many universities.

This book guides the reader through the mathematics, physics and practical techniques needed to use telescopes (from small amateur models to the larger instruments installed in many colleges) and to observe objects in the sky. Mathematics to around Advanced Placement standard (US) or A level (UK) is assumed, although High School Diploma (US) or GCSE-level (UK) mathematics plus some basic trigonometry will suffice most of the time. Most of the physics and engineering involved is described fully and requires no prior knowledge or experience.

This is a ‘how to’ book that provides the knowledge and background required to understand how and why telescopes work. Equipped with the techniques discussed in this book, the observer will be able to operate with confidence his or her telescope and to optimize its performance for a particular purpose. In principle the observer could calculate his or her own predictions of planetary positions (ephemerides), but more realistically the observer will be able to understand the published data lists properly instead of just treating them as ‘recipes.’ When the observer has obtained measurements, he/she will be able to analyze them in a scientific manner and to understand the significance and meaning of the results.

“Telescopes and Techniques, 3rd Edition” fills a niche at the start of an undergraduate astronomer’s university studies, as shown by it having been widely adopted as a set textbook. This third edition is now needed to update its material with the many new observing developments and study areas that have come into prominence since it was published. The book concentrates on the knowledge needed to understand how small(ish) optical telescopes function, their main designs and how to set them up, plus introducing the reader to the many ways in which objects in the sky change their positions and how they may be observed. Both visual and electronic imaging techniques are covered, together with an introduction to how data (measurements) should be processed and analyzed. A simple introduction to radio telescopes is also included. Brief coverage of the most advanced topics of photometry and spectroscopy are included, but mainly to enable the reader to see some of the developments possible from the basic observing techniques covered in the main parts of the book.
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